TA Instruments

AR1762-0001f

15/03/2013 16:53:07

Sample name	DI 40 mm AL P60
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1762
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 16:53:07

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99200	4.279	-18.992	10000	20.0	6.084	30.992	-6.190	5.348	-1.157	24790	1.7869	866.6	2.2336	223.36	3.411E-3	0.0	0.5
2.0080	10.02	13.462	10000	20.0	6.088	32.008	4.388	12.52	0.3503	24810	13.5621	158.1	16.953	1695.3	3.411E-3	0.0	0.5
2.9920	15.55	25.557	10000	20.0	6.089	32.992	8.330	19.44	0.4285	24810	27.0680	65.63	33.835	3383.5	3.411E-3	0.0	0.5
4.0320	18.48	34.017	10000	20.0	6.088	34.032	11.09	23.10	0.4801	24810	41.0238	46.51	51.280	5128.0	3.411E-3	0.1	0.6
4.9920	24.71	54.139	10000	20.0	6.086	34.992	17.65	30.89	0.5712	24800	67.7501	25.99	84.688	8468.8	3.411E-3	0.1	0.6
6.0000	31.62	82.227	10000	20.0	6.082	36.000	26.80	39.52	0.6782	24780	106.9910	15.87	133.74	13374	3.411E-3	0.1	0.6
7.0080	34.05	92.655	10000	20.0	6.079	37.008	30.20	42.57	0.7095	24770	126.4670	13.67	158.08	15808	3.411E-3	0.1	0.6
8.0080	39.32	117.86	10000	20.0	6.075	38.008	38.42	49.15	0.7815	24750	165.4140	10.24	206.77	20677	3.411E-3	0.1	0.6
9.0120	46.05	153.58	10000	20.0	6.066	39.012	50.06	57.56	0.8697	24720	223.3370	7.460	279.17	27917	3.411E-3	0.2	0.7
10.000	50.97	184.78	10000	20.0	6.060	40.000	60.23	63.71	0.9453	24690	274.9010	6.083	343.63	34363	3.411E-3	0.2	0.7
10.992	55.73	218.42	10000	20.0	6.051	40.992	71.19	69.67	1.022	24650	326.2100	5.080	407.76	40776	3.411E-3	0.2	0.7
12.008	60.11	250.70	10000	20.0	6.047	42.008	81.72	75.14	1.088	24640	379.1250	4.364	473.91	47391	3.411E-3	0.2	0.7
13.008	64.42	286.24	10000	20.0	6.038	43.008	93.30	80.52	1.159	24600	434.8650	3.794	543.58	54358	3.411E-3	0.2	0.7
14.008	69.16	324.86	10000	20.0	6.026	44.008	105.9	86.45	1.225	24550	498.6870	3.285	623.36	62336	3.411E-3	0.2	0.7
14.992	75.69	383.46	10000	20.0	6.011	44.992	125.0	94.61	1.321	24490	594.2700	2.736	742.84	74284	3.411E-3	0.2	0.7
15.992	79.93	428.19	10000	20.0	5.999	45.992	139.6	99.92	1.397	24440	664.3240	2.448	830.41	83041	3.411E-3	0.3	0.8
16.992	84.54	479.68	10000	20.0	5.984	46.992	156.4	105.7	1.480	24380	744.3000	2.184	930.38	93038	3.411E-3	0.3	0.8
18.008	90.99	547.74	10000	20.0	5.965	48.008	178.5	113.7	1.570	24300	855.5120	1.879	1069.4	1.0694E5	3.411E-3	0.3	0.8
19.008	95.04	591.27	10000	20.0	5.958	49.008	192.7	118.8	1.622	24270	931.1770	1.720	1164.0	1.1640E5	3.411E-3	0.3	0.8
20.008	99.40	645.28	10000	20.0	5.938	50.008	210.3	124.3	1.693	24190	1020.2900	1.567	1275.4	1.2754E5	3.411E-3	0.3	0.8
21.008	105.8	723.74	10000	20.0	5.912	51.008	235.9	132.3	1.783	24090	1153.2900	1.377	1441.6	1.4416E5	3.411E-3	0.4	0.9
22.008	109.9	778.63	10000	20.0	5.900	52.008	253.8	137.4	1.848	24040	1242.0500	1.274	1552.6	1.5526E5	3.411E-3	0.4	0.9
22.992	114.2	840.88	10000	20.0	5.887	52.992	274.1	142.8	1.919	23990	1343.4900	1.176	1679.4	1.6794E5	3.411E-3	0.4	0.9
24.000	120.6	920.74	10000	20.0	5.853	54.000	300.1	150.8	1.990	23850	1496.5300	1.049	1870.7	1.8707E5	3.411E-3	0.4	0.9
24.992	124.7	985.96	10000	20.0	5.831	54.992	321.4	155.9	2.061	23760	1596.8500	0.9774	1996.1	1.9961E5	3.411E-3	0.4	0.9
25.992	129.1	1044.0	10000	20.0	5.811	55.992	340.3	161.3	2.109	23680	1710.9100	0.9097	2138.6	2.1386E5	3.411E-3	0.4	0.9
27.016	135.5	1140.4	10000	20.0	5.783	57.016	371.7	169.3	2.195	23560	1881.8900	0.8219	2352.4	2.3524E5	3.411E-3	0.5	1.0
28.004	139.6	1203.1	10000	20.0	5.762	58.004	392.1	174.4	2.248	23480	1995.7900	0.7715	2494.7	2.4947E5	3.411E-3	0.5	1.0
28.992	143.6	1276.3	10000	20.0	5.733	58.992	416.0	179.6	2.317	23360	2116.2900	0.7245	2645.4	2.6454E5	3.411E-3	0.5	1.0
29.992	150.0	1398.7	10000	20.0	5.717	59.992	455.9	187.6	2.431	23290	2305.7300	0.6622	2882.2	2.8822E5	3.411E-3	0.5	1.0
31.008	154.1	1465.6	10000	20.0	5.698	61.008	477.7	192.7	2.479	23220	2432.2500	0.6253	3040.3	3.0403E5	3.411E-3	0.5	1.0
32.008	158.3	1545.3	10000	20.0	5.652	62.008	503.7	197.8	2.546	23030	2635.9500	0.5883	3294.9	3.2949E5	3.411E-3	0.5	1.0
32.992	164.7	1650.1	10000	20.0	5.624	62.992	537.8	205.8	2.613	22910	2773.6499	0.5409	3467.1	3.4671E5	3.411E-3	0.5	1.0
33.992	168.8	1724.0	10000	20.0	5.600	63.992	561.9	211.0	2.663	22820	2912.7700	0.5126	3641.0	3.6410E5	3.411E-3	0.6	1.1
34.992	174.9	1854.2	10000	20.0	5.568	64.992	604.4	218.6	2.765	22690	3127.4900	0.4748	3909.4	3.9094E5	3.411E-3	0.6	1.1
36.008	179.1	1946.6	10000	20.0	5.515	66.008	634.5	223.9	2.834	22470	3279.1799	0.4483	4099.0	4.0990E5	3.411E-3	0.6	1.1
37.008	183.3	2010.4	10000	20.0	5.477	67.008	655.3	229.1	2.860	22320	3430.7500	0.4253	4288.4	4.2884E5	3.411E-3	0.6	1.1
37.992	189.3	2161.7	10000	20.0	5.474	67.992	704.6	236.6	2.978	22300	3658.1101	0.3983	4572.6	4.5726E5	3.411E-3	0.6	1.1
39.008	193.5	2236.3	10000	20.0	5.414	69.008	728.9	241.8	3.014	22060	3822.2500	0.3772	4777.8	4.7778E5	3.411E-3	0.7	1.2
40.008	199.7	2375.5	10000	20.0	5.382	70.008	774.3	249.6	3.102	21930	4068.5801	0.3521	5085.7	5.0857E5	3.411E-3	0.7	1.2
41.008	203.7	2468.7	10000	20.0	5.375	71.008	804.7	254.6	3.160	21900	4232.7002	0.3378	5290.9	5.2909E5	3.411E-3	0.7	1.2
42.004	207.9	2549.7	10000	20.0	5.311	72.004	831.1	259.8	3.198	21640	4409.5601	0.3205	5512.0	5.5120E5	3.411E-3	0.7	1.2
43.004	214.1	2690.9	10000	20.0	5.261	73.004	877.1	267.6	3.278	21440	4674.2900	0.2993	5842.9	5.8429E5	3.411E-3	0.7	1.2
44.008	218.1	2790.5	10000	20.0	5.230	74.008	909.6	272.7	3.336	21310	4851.0601	0.2866	6063.8	6.0638E5	3.411E-3	0.7	1.2
45.008	224.3	2934.1	10000	20.0	5.202	75.008	956.4	280.4	3.411	21200	5130.9800	0.2697	6413.7	6.4137E5	3.411E-3	0.8	1.3
45.996	228.4	3045.0	10000	20.0	5.148	75.996	992.5	285.5	3.477	20980	5318.4702	0.2574	6648.1	6.6481E5	3.411E-3	0.8	1.3
46.992	234.5	3201.6	10000	20.0	5.101	76.992	1044	293.1	3.560	20780	5603.2300	0.2419	7004.0	7.0040E5	3.411E-3	0.8	1.3
47.996	238.5	3314.7	10000	20.0	5.054	77.996	1080	298.1	3.624	20590	5797.2100	0.2317	7246.5	7.2465E5	3.411E-3	0.8	1.3
48.992	242.6	3436.0	10000	20.0	4.997	78.992	1120	303.3	3.693	20360	5999.2300	0.2213	7499.0	7.4990E5	3.411E-3	0.8	1.3
50.004	248.8	3584.4	10000	20.0	4.956	80.004	1168	311.0	3.757	20190	6301.9702	0.2088	7877.5	7.8775E5	3.411E-3	0.8	1.3
51.004	252.8	3665.3	10000	20.0	4.909	81.004	1195	316.0	3.780	20000	6510.1699	0.2003	8137.7	8.1377E5	3.411E-3	0.9	1.4
51.992	259.0	3873.4	10000	20.0	4.848	81.992	1263	323.8	3.899	19750	6832.1201	0.1884	8540.2	8.5402E5	3.411E-3	0.9	1.4
53.000	263.1	3979.1	10000	20.0	4.785	83.000	1297	328.9	3.944	19490	7047.2100	0.1802	8809.0	8.8090E5	3.411E-3	0.9	1.4
54.004	269.1	4157.1	10000	20.0	4.707	84.004	1355	336.4	4.028	19180	7374.1802	0.1695	9217.7	9.2177E5	3.411E-3	0.9	1.4
55.004	273.3	4303.4	10000	20.0	4.761	85.004	1403	341.6	4.107	19400	7603.1201	0.1663	9503.9	9.5039E5	3.411E-3	0.9	1.4
56.004	277.3	4398.9	10000	20.0	4.697	86.004	1434	346.7	4.136	19140	7828.0601	0.1592	9785.1	9.7851E5	3.411E-3	0.9	1.4
57.048	283.4	4577.5	10000	20.0	4.616	87.048	1492	354.2	4.212	18810	8168.3799	0.1499	10210	1.0210E6	3.411E-3	1.0	1.5
58.004	287.5	4709.9	10000	20.0	4.508	88.004	1535	359.3	4.272	18370	8408.2305	0.1423	10510	1.0510E6	3.411E-3	1.0	1.5
58.988	293.6	4924.6	10000	20.0	4.479	88.988	1605	367.0	4.374	18250	8771.7500	0.1355	10965	1.0965E6	3.411E-3	1.0	1.5
59.988	297.6	5013.1	10000	20.0	4.384	89.988	1634	372.0	4.392	17860	9010.1396	0.1291	11263	1.1263E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0280	300.0	5090.0	10000	20.0	4.388	91.028	1659	375.0	4.424	17880	314.9530	0.1271	393.69	39369	3.411E-3	0.0	1.5
2.0480	300.0	5079.3	10000	20.0	4.408	92.048	1656	375.0	4.415	17960	563.1220	0.1277	703.90	70390	3.411E-3	0.0	1.5
3.0160	300.0	5095.5	10000	20.0	4.429	93.016	1661	375.0	4.429	18040	814.2870	0.1283	1017.9	1.0179E5	3.411E-3	0.1	1.6
4.0080	300.0	5096.4	10000	20.0	4.402	94.008	1661	375.0	4.430	17940	1191.4301	0.1275	1489.3	1.4893E5	3.411E-3	0.1	1.6
5.0200	300.0	5067.0	10000	20.0	4.425	95.020	1652	375.0	4.404	18030	1442.6500	0.1282	1803.3	1.8033E5	3.411E-3	0.1	1.6
6.0880	300.0	5083.5	10000	20.0	4.347	96.088	1657	375.0	4.418	17710	1819.7500	0.1259	2274.7	2.2747E5	3.411E-3	0.1	1.6
7.0040	300.0	5099.4	10000	20.0	4.410	97.004	1662	375.0	4.432	17970	2072.6699	0.1278	2590.8	2.5908E5	3.411E-3	0.1	1.6
8.0160	300.0	5116.1	10000	20.0	4.448	98.016	1668	375.0	4.447	18120	2322.9800	0.1289	2903.7	2.9037E5	3.411E-3	0.1	1.6
9.0400	300.0	5083.4	10000	20.0	4.420	99.040	1657	375.0	4.418	18010	2700.8401	0.1280	3376.1	3.3761E5	3.411E-3	0.2	1.7
10.016	300.0	5111.5	10000	20.0	4.399	100.016	1666	375.0	4.443	17920	2950.7700	0.1274	3688.5	3.6885E5	3.411E-3	0.2	1.7
11.016	300.0	5061.2	10000	20.0	4.392	101.016	1650	375.0	4.399	17890	3330.7000	0.1272	4163.4	4.1634E5	3.411E-3	0.2	1.7
12.020	300.0	5064.9	10000	20.0	4.385	102.020	1651	375.0	4.403	17870	3579.0801	0.1271	4473.9	4.4739E5	3.411E-3	0.2	1.7
13.016	300.0	5089.2	10000	20.0	4.378	103.016	1659	375.0	4.424	17840	3830.4500	0.1269	4788.1	4.7881E5	3.411E-3	0.2	1.7
14.016	300.0	5118.9	10000	20.0	4.449	104.016	1669	375.0	4.449	18130	4207.3799	0.1289	5259.2	5.2592E5	3.411E-3	0.2	1.7
15.016	300.0	5093.6	10000	20.0	4.397	105.016	1660	375.0	4.427	17920	4459.4199	0.1274	5574.3	5.5743E5	3.411E-3	0.3	1.8
16.000	300.0	5125.9	10000	20.0	4.431	106.000	1671	375.0	4.456	18050	4709.9102	0.1284	5887.4	5.8874E5	3.411E-3	0.3	1.8
17.020	300.0	5149.6	10000	20.0	4.469	107.020	1679	375.0	4.476	18210	5089.4199	0.1295	6361.8	6.3618E5	3.411E-3	0.3	1.8
18.000	300.0	5071.1	10000	20.0	4.402	108.000	1653	375.0	4.407	17940	5339.3799	0.1275	6674.2	6.6742E5	3.411E-3	0.3	1.8
19.048	300.0	5108.0	10000	20.0	4.479	109.048	1665	375.0	4.440	18250	5715.2598	0.1298	7144.1	7.1441E5	3.411E-3	0.3	1.8
20.020	300.0	5072.6	10000	20.0	4.445	110.020	1653	375.0	4.409	18110	5971.8501	0.1288	7464.8	7.4648E5	3.411E-3	0.3	1.8
21.020	300.0	5125.9	10000	20.0	4.407	111.020	1671	375.0	4.456	17960	6217.9102	0.1277	7772.4	7.7724E5	3.411E-3	0.4	1.9
22.040	300.0	5102.1	10000	20.0	4.416	112.040	1663	375.0	4.435	17990	6594.8701	0.1279	8243.6	8.2436E5	3.411E-3	0.4	1.9
23.000	300.0	5106.6	10000	20.0	4.379	113.000	1664	375.0	4.439	17840	6846.3198	0.1269	8557.9	8.5579E5	3.411E-3	0.4	1.9
24.016	300.0	5112.3	10000	20.0	4.458	114.016	1666	375.0	4.444	18160	7224.6602	0.1292	9030.8	9.0308E5	3.411E-3	0.4	1.9
25.016	300.0	5093.7	10000	20.0	4.412	115.016	1660	375.0	4.427	17980	7474.7900	0.1278	9343.5	9.3435E5	3.411E-3	0.4	1.9
26.016	300.0	5082.9	10000	20.0	4.405	116.016	1657	375.0	4.418	17950	7725.9399	0.1276	9657.4	9.6574E5	3.411E-3	0.4	1.9
27.024	300.0	5129.8	10000	20.0	4.487	117.024	1672	375.0	4.459	18280	8104.1401	0.1300	10130	1.0130E6	3.411E-3	0.5	2.0
28.000	300.0	5104.3	10000	20.0	4.417	118.000	1664	375.0	4.437	18000	8355.4102	0.1280	10444	1.0444E6	3.411E-3	0.5	2.0
29.016	300.0	5114.3	10000	20.0	4.475	119.016	1667	375.0	4.445	18230	8605.5098	0.1296	10757	1.0757E6	3.411E-3	0.5	2.0
30.000	300.0	5079.5	10000	20.0	4.413	120.000	1656	375.0	4.415	17980	8982.5195	0.1278	11228	1.1228E6	3.411E-3	0.5	2.0
31.024	300.0	5134.0	10000	20.0	4.557	121.024	1673	375.0	4.463	18570	9233.9199	0.1320	11542	1.1542E6	3.411E-3	0.5	2.0
32.004	300.0	5127.6	10000	20.0	4.502	122.004	1671	375.0	4.457	18340	9610.7998	0.1304	12014	1.2014E6	3.411E-3	0.5	2.0
33.028	300.0	5119.6	10000	20.0	4.449	123.028	1669	375.0	4.450	18130	9862.2803	0.1289	12328	1.2328E6	3.411E-3	0.6	2.1
34.016	300.0	5085.0	10000	20.0	4.444	124.016	1657	375.0	4.420	18110	10113.500	0.1287	12642	1.2642E6	3.411E-3	0.6	2.1
35.016	300.0	5132.0	10000	20.0	4.517	125.016	1673	375.0	4.461	18410	10490.400	0.1309	13113	1.3113E6	3.411E-3	0.6	2.1
36.000	300.0	5104.2	10000	20.0	4.427	126.000	1664	375.0	4.436	18040	10741.900	0.1283	13427	1.3427E6	3.411E-3	0.6	2.1
37.000	300.0	5149.3	10000	20.0	4.423	127.000	1678	375.0	4.475	18020	11121.400	0.1281	13902	1.3902E6	3.411E-3	0.6	2.1
38.016	300.0	5091.0	10000	20.0	4.394	128.016	1659	375.0	4.425	17900	11370.100	0.1273	14213	1.4213E6	3.411E-3	0.6	2.1
39.016	300.0	5138.8	10000	20.0	4.552	129.016	1675	375.0	4.467	18550	11621.400	0.1319	14527	1.4527E6	3.411E-3	0.7	2.2
40.016	300.0	5148.8	10000	20.0	4.467	130.016	1678	375.0	4.475	18200	11998.400	0.1294	14998	1.4998E6	3.411E-3	0.7	2.2
41.000	300.0	5134.7	10000	20.0	4.454	131.000	1674	375.0	4.463	18150	12251.400	0.1291	15314	1.5314E6	3.411E-3	0.7	2.2
42.024	300.0	5130.0	10000	20.0	4.419	132.024	1672	375.0	4.459	18000	12629.700	0.1280	15787	1.5787E6	3.411E-3	0.7	2.2
43.016	300.0	5087.8	10000	20.0	4.436	133.016	1658	375.0	4.422	18070	12880.500	0.1285	16101	1.6101E6	3.411E-3	0.7	2.2
44.008	300.0	5091.8	10000	20.0	4.426	134.008	1660	375.0	4.426	18040	13131.300	0.1283	16414	1.6414E6	3.411E-3	0.7	2.2
45.000	300.0	5144.8	10000	20.0	4.454	135.000	1677	375.0	4.472	18150	13508.700	0.1290	16886	1.6886E6	3.411E-3	0.8	2.3
46.040	300.0	5154.2	10000	20.0	4.484	136.040	1680	375.0	4.480	18270	13759.000	0.1299	17199	1.7199E6	3.411E-3	0.8	2.3
47.000	300.0	5095.0	10000	20.0	4.381	137.000	1661	375.0	4.428	17850	14014.200	0.1269	17518	1.7518E6	3.411E-3	0.8	2.3
48.000	300.0	5123.2	10000	20.0	4.459	138.000	1670	375.0	4.453	18170	14386.100	0.1292	17983	1.7983E6	3.411E-3	0.8	2.3
49.012	300.0	5123.9	10000	20.0	4.458	139.012	1670	375.0	4.454	18160	14637.400	0.1292	18297	1.8297E6	3.411E-3	0.8	2.3
50.016	300.0	5132.5	10000	20.0	4.427	140.016	1673	375.0	4.461	18040	15014.400	0.1283	18768	1.8768E6	3.411E-3	0.8	2.3
51.016	300.0	5157.9	10000	20.0	4.525	141.016	1681	375.0	4.483	18440	15265.700	0.1311	19082	1.9082E6	3.411E-3	0.9	2.4
52.024	300.0	5121.4	10000	20.0	4.474	142.024	1669	375.0	4.451	18230	15517.000	0.1296	19396	1.9396E6	3.411E-3	0.9	2.4
53.004	300.0	5114.4	10000	20.0	4.407	143.004	1667	375.0	4.446	17950	15894.000	0.1277	19868	1.9868E6	3.411E-3	0.9	2.4
54.044	300.0	5100.3	10000	20.0	4.372	144.044	1662	375.0	4.433	17810	16145.900	0.1267	20182	2.0182E6	3.411E-3	0.9	2.4
55.016	300.0	5110.7	10000	20.0	4.449	145.016	1666	375.0	4.442	18130	16524.699	0.1289	20656	2.0656E6	3.411E-3	0.9	2.4
56.016	300.0	5116.3	10000	20.0	4.440	146.016	1668	375.0	4.447	18090	16773.801	0.1286	20967	2.0967E6	3.411E-3	0.9	2.4
57.000	300.0	5148.2	10000	20.0	4.414	147.000	1678	375.0	4.475	17980	17025.000	0.1279	21281	2.1281E6	3.411E-3	1.0	2.5
58.000	300.0	5125.4	10000	20.0	4.435	148.000	1671	375.0	4.455	18070	17402.100	0.1285	21753	2.1753E6	3.411E-3	1.0	2.5
59.016	300.0	5136.9	10000	20.0	4.439	149.016	1674	375.0	4.465	18090	17653.400	0.1286	22067	2.2067E6	3.411E-3	1.0	2.5
60.000	300.0	5110.5	10000	20.0	4.447	150.000	1666	375.0	4.442	18120	17904.699	0.1288	22381	2.2381E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	296.0	5049.9	10000	20.0	4.532	152.004	1646	369.9	4.449	18460	329.4750	0.1349	411.84	41184	3.411E-3	0.0	2.5
1.9960	292.0	4824.8	10000	20.0	4.500	152.996	1573	365.0	4.309	18330	577.5180	0.1376	721.90	72190	3.411E-3	0.0	2.5
3.0000	287.9	4709.8	10000	20.0	4.570	154.000	1535	359.9	4.266	18620	804.4640	0.1438	1005.6	1.0056E5	3.411E-3	0.1	2.6
4.0000	281.8	4536.5	10000	20.0	4.662	155.000	1479	352.2	4.198	19000	1154.3600	0.1531	1443.0	1.4430E5	3.411E-3	0.1	2.6
5.0080	277.8	4381.1	10000	20.0	4.671	156.008	1428	347.2	4.113	19030	1379.5500	0.1578	1724.4	1.7244E5	3.411E-3	0.1	2.6
6.0200	271.7	4254.2	10000	20.0	4.781	157.020	1387	339.6	4.083	19480	1717.4700	0.1689	2146.8	2.1468E5	3.411E-3	0.1	2.6
7.0000	267.5	4116.7	10000	20.0	4.796	158.000	1342	334.4	4.012	19540	1942.7800	0.1747	2428.5	2.4285E5	3.411E-3	0.1	2.6
7.9920	261.5	3925.7	10000	20.0	4.838	158.992	1280	326.9	3.914	19710	2262.0901	0.1845	2827.6	2.8276E5	3.411E-3	0.1	2.6
9.0000	257.4	3815.4	10000	20.0	4.902	160.000	1244	321.8	3.865	19970	2474.8101	0.1929	3093.5	3.0935E5	3.411E-3	0.2	2.7
9.9960	253.3	3689.4	10000	20.0	4.903	160.996	1203	316.7	3.798	19980	2689.1799	0.1992	3361.5	3.3615E5	3.411E-3	0.2	2.7
10.996	247.2	3514.8	10000	20.0	4.951	161.996	1146	309.0	3.708	20170	2995.3601	0.2113	3744.2	3.7442E5	3.411E-3	0.2	2.7
12.000	243.1	3449.6	10000	20.0	5.022	163.000	1124	303.9	3.699	20460	3194.9299	0.2215	3993.7	3.9937E5	3.411E-3	0.2	2.7
12.996	236.9	3284.7	10000	20.0	5.064	163.996	1071	296.2	3.615	20630	3495.2100	0.2352	4369.0	4.3690E5	3.411E-3	0.2	2.7
13.996	232.8	3155.1	10000	20.0	5.124	164.996	1028	291.0	3.534	20880	3690.7700	0.2466	4613.5	4.6135E5	3.411E-3	0.2	2.7
14.996	228.8	3057.3	10000	20.0	5.156	165.996	996.5	286.0	3.485	21010	3972.3799	0.2569	4965.5	4.9655E5	3.411E-3	0.2	2.8
16.000	222.6	2884.2	10000	20.0	5.172	167.000	940.1	278.3	3.378	21070	4159.2402	0.2721	5199.1	5.1991E5	3.411E-3	0.3	2.8
16.996	218.4	2789.9	10000	20.0	5.221	167.996	909.4	273.0	3.330	21270	4340.5898	0.2854	5425.7	5.4257E5	3.411E-3	0.3	2.8
18.000	212.4	2661.5	10000	20.0	5.261	169.000	867.5	265.5	3.268	21440	4602.5098	0.3041	5753.1	5.7531E5	3.411E-3	0.3	2.8
18.996	208.3	2565.8	10000	20.0	5.306	169.996	836.3	260.4	3.212	21620	4778.4302	0.3189	5973.0	5.9730E5	3.411E-3	0.3	2.8
19.996	202.0	2416.3	10000	20.0	5.366	170.996	787.6	252.6	3.118	21860	5035.6401	0.3428	6294.6	6.2946E5	3.411E-3	0.3	2.8
21.000	198.0	2324.5	10000	20.0	5.382	172.000	757.7	247.5	3.061	21930	5196.7402	0.3580	6495.9	6.4959E5	3.411E-3	0.4	2.9
21.992	193.9	2222.6	10000	20.0	5.405	172.992	724.4	242.4	2.989	22020	5359.2002	0.3749	6699.0	6.6990E5	3.411E-3	0.4	2.9
22.996	187.6	2094.8	10000	20.0	5.473	173.996	682.8	234.5	2.912	22300	5603.3901	0.4056	7004.2	7.0042E5	3.411E-3	0.4	2.9
23.996	183.5	2019.1	10000	20.0	5.485	174.996	658.1	229.3	2.869	22350	5752.8901	0.4249	7191.1	7.1911E5	3.411E-3	0.4	2.9
25.084	177.3	1887.2	10000	20.0	5.530	176.084	615.1	221.6	2.776	22530	5977.8301	0.4587	7472.3	7.4723E5	3.411E-3	0.4	2.9
26.000	173.1	1794.8	10000	20.0	5.556	177.000	585.0	216.3	2.704	22640	6128.5000	0.4837	7660.6	7.6606E5	3.411E-3	0.4	3.0
26.996	169.0	1709.0	10000	20.0	5.585	177.996	557.1	211.2	2.637	22760	6266.3398	0.5100	7832.9	7.8329E5	3.411E-3	0.4	3.0
27.996	162.8	1599.1	10000	20.0	5.624	178.996	521.2	203.6	2.561	22910	6472.5498	0.5530	8090.7	8.0907E5	3.411E-3	0.5	3.0
28.996	158.6	1531.2	10000	20.0	5.673	179.996	499.1	198.3	2.517	23110	6610.1201	0.5880	8262.7	8.2627E5	3.411E-3	0.5	3.0
29.996	154.3	1458.7	10000	20.0	5.693	180.996	475.5	192.9	2.464	23190	6748.2998	0.6231	8435.4	8.4354E5	3.411E-3	0.5	3.0
30.996	148.2	1341.2	10000	20.0	5.714	181.996	437.2	185.3	2.359	23280	6928.1699	0.6780	8660.2	8.6602E5	3.411E-3	0.5	3.0
31.996	144.0	1275.7	10000	20.0	5.746	182.996	415.8	180.0	2.310	23410	7052.9199	0.7227	8816.2	8.8162E5	3.411E-3	0.5	3.0
33.000	137.7	1168.3	10000	20.0	5.777	184.000	380.8	172.2	2.212	23540	7227.7598	0.7939	9034.7	9.0347E5	3.411E-3	0.6	3.1
33.996	133.6	1096.2	10000	20.0	5.783	184.996	357.3	167.1	2.139	23560	7339.8398	0.8443	9174.8	9.1748E5	3.411E-3	0.6	3.1
34.996	129.4	1037.8	10000	20.0	5.817	185.996	338.3	161.8	2.091	23700	7451.5498	0.9056	9314.4	9.3144E5	3.411E-3	0.6	3.1
36.000	122.9	940.71	10000	20.0	5.848	187.000	306.6	153.7	1.995	23830	7614.2998	1.009	9517.9	9.5179E5	3.411E-3	0.6	3.1
37.000	118.8	884.02	10000	20.0	5.865	188.000	288.1	148.6	1.940	23890	7713.5000	1.083	9641.9	9.6419E5	3.411E-3	0.6	3.1
37.996	114.6	830.31	10000	20.0	5.877	188.996	270.6	143.3	1.889	23950	7813.7300	1.166	9767.2	9.7672E5	3.411E-3	0.6	3.1
38.996	108.1	734.34	10000	20.0	5.902	189.996	239.4	135.1	1.771	24050	7956.3101	1.317	9945.4	9.9454E5	3.411E-3	0.6	3.2
40.000	104.0	680.18	10000	20.0	5.920	191.000	221.7	130.1	1.705	24120	8043.9600	1.426	10055	1.0055E6	3.411E-3	0.7	3.2
40.996	99.81	631.82	10000	20.0	5.937	191.996	205.9	124.8	1.651	24190	8130.6499	1.554	10163	1.0163E6	3.411E-3	0.7	3.2
41.996	93.28	549.00	10000	20.0	5.954	192.996	178.9	116.6	1.535	24260	8255.3096	1.784	10319	1.0319E6	3.411E-3	0.7	3.2
43.012	89.22	504.25	10000	20.0	5.972	194.012	164.4	111.5	1.474	24330	8329.5898	1.956	10412	1.0412E6	3.411E-3	0.7	3.2
43.996	84.99	462.93	10000	20.0	5.977	194.996	150.9	106.2	1.420	24350	8404.0703	2.158	10505	1.0505E6	3.411E-3	0.7	3.2
44.996	80.53	421.57	10000	20.0	5.996	195.996	137.4	100.7	1.365	24430	8478.5098	2.411	10598	1.0598E6	3.411E-3	0.7	3.3
45.996	73.98	350.94	10000	20.0	6.013	196.996	114.4	92.47	1.237	24500	8578.0195	2.865	10723	1.0723E6	3.411E-3	0.8	3.3
47.000	69.70	311.62	10000	20.0	6.021	198.000	101.6	87.13	1.166	24530	8639.6602	3.231	10800	1.0800E6	3.411E-3	0.8	3.3
48.000	65.16	276.71	10000	20.0	6.033	199.000	90.19	81.45	1.107	24580	8701.4805	3.705	10877	1.0877E6	3.411E-3	0.8	3.3
49.004	60.54	238.59	10000	20.0	6.037	200.004	77.77	75.68	1.028	24600	8784.0098	4.295	10980	1.0980E6	3.411E-3	0.8	3.3
49.996	54.13	196.41	10000	20.0	6.052	200.996	64.02	67.67	0.9461	24660	8831.1396	5.386	11039	1.1039E6	3.411E-3	0.8	3.3
50.996	49.42	164.56	10000	20.0	6.057	201.996	53.64	61.78	0.8682	24680	8880.5996	6.466	11101	1.1101E6	3.411E-3	0.8	3.4
51.996	44.58	138.57	10000	20.0	6.062	202.996	45.17	55.73	0.8105	24700	8923.4404	7.953	11154	1.1154E6	3.411E-3	0.9	3.4
52.992	40.28	116.36	10000	20.0	6.068	203.992	37.93	50.35	0.7533	24720	8960.1602	9.753	11200	1.1200E6	3.411E-3	0.9	3.4
53.996	35.49	93.121	10000	20.0	6.076	204.996	30.35	44.36	0.6842	24760	8996.5801	12.58	11246	1.1246E6	3.411E-3	0.9	3.4
54.996	30.49	70.515	10000	20.0	6.079	205.996	22.98	38.11	0.6031	24770	9026.8896	17.05	11284	1.1284E6	3.411E-3	0.9	3.4
55.996	26.24	53.727	10000	20.0	6.084	206.996	17.51	32.80	0.5339	24790	9051.0898	23.04	11314	1.1314E6	3.411E-3	0.9	3.4
56.992	21.23	37.449	10000	20.0	6.085	207.992	12.21	26.54	0.4599	24790	9074.8701	35.19	11344	1.1344E6	3.411E-3	0.9	3.5
58.004	14.84	19.568	10000	20.0	6.086	209.004	6.378	18.55	0.3439	24800	9097.6396	72.08	11372	1.1372E6	3.411E-3	1.0	3.5
58.996	11.76	12.588	10000	20.0	6.088	209.996	4.103	14.70	0.2790	24810	9103.3604	114.7	11379	1.1379E6	3.411E-3	1.0	3.5
60.000	6.558	3.5824	10000	20.0	6.092	211.000	1.168	8.198	0.1424	24820	9111.5000	369.3	11389	1.1389E6	3.411E-3	1.0	3.5

